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TRIORTHOCRESYL PHOSPHATE: METHOD 5037, Issue 1, dated 15 August 1994 - Page 4 of 4 REFERENCES: [1] Backup Data Report for Triorthocresyl Phosphate, in Documentation of the NIOSH Validation Tests, prepared under NIOSH Contract CDC-99-74-45 (1977). [2] NIOSH Manual of Analytical Methods, 2nd. ed., V. 3, S209, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-157-C (1977). [3] Willis, T., Optimizing the Quantitative Gas Chromatographic Analysis of Aryl Phosphate Isomers, LC-GC, 11(7):510 (1993). [4] Willis, T., and Hathaway, R., Structural Influences on the Separation of Aryl Phosphate Isomers Using Wide-Bore Capillary Gas Chromatography, LC-GC, 9(3):220 (1991). [5] Krishnamurthy, M., Rajalakshmi, S., and Kapur, O., Detection of Tricresyl Phosphates and Determination of Tri-o-Cresyl Phosphate in Edible Oils, J. Assoc. Off. Anal. Chem., 68 (6): 1074 (1985). [6] Ishikawa, S., Taketomi, M., and Shinohara, R., Determination of Trialkyl and Triaryl Phosphates in Environmental Samples, Water Res., 19 (1): 119 (1985). [7] Nomeir, A., and Abou-Donia, M., High-Performance Liquid-Chromatographic Analysis on RadialCompression Column of the Neurotoxic Tri-o-Cresyl [Tri-o-Tolyl] Phosphate and Metabolites, Anal. Biochem. , 135 (2): 296 (1983). [8] Barceló, D., Application of Thermospray Liquid Chromatography/Mass Spectrometry for Determination of Organophosphorus Pesticides and Trialkyl and Triaryl Phosphates, Biomed. Environ. Mass Spectrom. , 17 (5): 363 (1988). [9] Barceló, D., Maris, F., Frei, R., de Jong, G., and Brinkman, U., Determination of Trialkyl and Triaryl Phosphates by Narrow-Bore Liquid Chromatography with on-line Thermionic Detection, Intern. J. Environ. Anal. Chem., 30 (1-2): 95 (1987). [10] Chowdhury, B., Nandy, A., Saha, C., Podder, G., Sarkar, S., Saha, D., Chakraborty, S., Chatterjee, H., and Roy, P., Determination of Tricresyl Phosphate in Edible Oil by HPLC Method, J. Inst. Chem. (India), 60 (5): 197 (1988). [11] Chen, S., Analysis of the Ortho Isomer of Tricresyl Phosphate in Commercial Tricresyl Phosphate Additives, Report, BRDEC-2448; Order No. AD-A183489, 26 pp. Avail. NTIS from: Gov. Rep. Announce. Index (U.S.) 1987, 87 (23), Abstr. No. 754,470. [12] Material Safety Data Sheet for Diethyl Ether, No. 343, General Electric Company, Schenectady, N.Y., August, 1979. [13] Material Safety Data Sheet for Tricresyl Phosphate, No. 332, General Electric Company, Schenectady, N.Y., November, 1977. [14] Material Safety Data Sheet for Tricresyl Phosphate, No. T5161, J.T. Baker Chemical Company, Phillipsburg, N.J., May 1, 1989.

METHOD REVISED BY: Robert P. Streicher, Ph.D., NIOSH/DPSE.

NIOSH Manual of Analytical Methods (NMAM), Fourth Edition, 8/15/94